Home Chemical • Download Chemical Physics of Intercalation by Albert Hérold (auth.), A. P. Legrand, S. Flandrois (eds.) PDF

Download Chemical Physics of Intercalation by Albert Hérold (auth.), A. P. Legrand, S. Flandrois (eds.) PDF

By Albert Hérold (auth.), A. P. Legrand, S. Flandrois (eds.)

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About at the same time Selig and coworkers have intercalated fluorine in the presense of HF, AsF5, or BF3' Compounds of stage 5 to 1 have been synthetised. The interplanar distance of 605 pm is close to that of 670 pm measured in the graphite-chlorine compounds except at the 1st stage compounds in which the value of 1100 pm corresponds to a double layer of fluorine atoms [53]. More recently intercalation of pure fluorine has been carried out by Touhara [54]. A period of 3-6 months is required for the synthesis of CxF compounds ( 6 < x ~ 14).

J. Rouxel, idem 5. W. Rudorff, U. Hofmann, Z. electrochem. 40 (1934) 511 6. W. RGdorff, U. Hofmann, Z. Anorg. Allg. Chern. 288 (1938)1 7. G. Hennig, J. Chern. Phys. 19 (1951)922 8. L. Dzurus, G. Hennig, J. Am. Chern. Soc. 79 (1957) 5897 9. R. C. R. Ubbelohde, J. Chern. Soc, London (1951)191 10. R. Setton, Bull. Soc. Chim. Fr. (1960)1758 11. J. Salzano, S. Aronson J. Chern. Phys. 45(1966)2221 12. M. Armand, These, Grenoble (1978) 13. D. Crowell, J. Chern. Phys. 8 (1954)1397 14. N. Daumas, A. R. Acad.

According to analytical and spectroscopical data, intercalated species are SnCl~- ions associated with solvent molecules. V. radiations in different solvents the best being the mixture Sn(CH3)4 + SnC14 + CC1 4 [34, 36]. Intercalated species seem to be oligomeric ions such as {Cl-Sn(CH 3)3-[C1-(CH 3)3]n-Cl }Photochemical insertion of iron carbonyls [37, 38] Fe(CO)5' FeZ(CO)3' Fe3(CO)IZ in different solvents (THF, benzene, hexane) also led to mixtures of stages and intercalated layers containing carbonyls and solvent molecules.

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